机器人实现实时样品操控,突破同步辐射实验限制
Multi-Tool Robotics Enables In-Situ Sample Manipulation for Time-Resolved Synchrotron Measurements

- 多工具模块化机器人平台,可在实验舱内自主操作样品
- 首次实现钙钛矿薄膜中瞬态原位动态的实时观测
- 适合需要高通量、自动化同步辐射实验的研究者
同步辐射光束线的高通量光子可探测快速动力学过程。然而,辐射安全规程禁止实验过程中人工介入,限制了连续数据采集期间多样化的实时样品操作。本文在X射线散射光束线上搭建了一套机器人平台,实现了实验舱内实时样品处理与操控,揭示了钙钛矿薄膜中此前无法获取的瞬态原位动态。该模块化多工具机器人架构突破了人类可达性限制,为自动化与自主同步辐射实验奠定了基础。
原文摘要 · Abstract (English)
The high photon flux at synchrotron beamlines allows for the measurement of fast dynamical processes. However, beamline radiation-safety protocols prohibit human intervention during X-ray experiments, limiting the ability to perform versatile real-time sample manipulations during continuous data acquisition. Here we present a robotic platform at an X-ray scattering beamline to enable real-time sample handling and processing in the experimental hutch, revealing previously inaccessible transient in-situ dynamics in perovskite thin films. This modular multi-tool robotic architecture enables in-hutch sample manipulation beyond human-access constraints, establishing a foundation for automated and autonomous synchrotron experimentation.
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